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calculate the theoretical yield of the final product in the reaction

calculate the theoretical yield of the final product in the reaction

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Please help me calculate the theoretical yield of the final product in the reaction shown in the photo!
Synthesis of cyclopentadienyliron dicarbonyl iodide Procedure A 50 mL one neck round bottom flask equipped with a refluxing condenser is charged with 2.0 g of [(15-C5H5) Fe(CO)2]2 and 25 mL of chloroform followed by 2.0 g of iodine. This black/brown mixture is refluxed for 30 minutes under N2 atmosphere (use an oil bath, nitrogen bubbler and a refluxing condenser). After cooling to room temperature, the reaction mixture is washed in a separatory funnel with a solution of sodium thiosulfate 5-hydrate (10 g in 50 mL of H2O or scale up as necessary) in two or three portions to remove excess iodine. Remove the volatiles using a rotary evaporator. The black crystalline residue was washed with petroleum ether (2 x 5 mL) and sucked dry to obtain the final product, (n5-C5H5) Fe(CO)21. Record the IR spectra of both the starting material and the final product.
Transcribed Image Text:Synthesis of cyclopentadienyliron dicarbonyl iodide Procedure A 50 mL one neck round bottom flask equipped with a refluxing condenser is charged with 2.0 g of [(15-C5H5) Fe(CO)2]2 and 25 mL of chloroform followed by 2.0 g of iodine. This black/brown mixture is refluxed for 30 minutes under N2 atmosphere (use an oil bath, nitrogen bubbler and a refluxing condenser). After cooling to room temperature, the reaction mixture is washed in a separatory funnel with a solution of sodium thiosulfate 5-hydrate (10 g in 50 mL of H2O or scale up as necessary) in two or three portions to remove excess iodine. Remove the volatiles using a rotary evaporator. The black crystalline residue was washed with petroleum ether (2 x 5 mL) and sucked dry to obtain the final product, (n5-C5H5) Fe(CO)21. Record the IR spectra of both the starting material and the final product.
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