An ore containing magnetite, Fe3O4 was analyzed by dissolving a 1.5419 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 0.8525 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample.

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
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An ore containing magnetite, Fe3O4 was analyzed by dissolving a 1.5419 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 0.8525 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample.

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