An ore containing magnetite, Fe3O4, was analysed by dissolving a 4.9 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 2.8 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample (Fe3O4 =231.54 g/mol, Fe2O3 = 159.69 g/mol)

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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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An ore containing magnetite, Fe3O4, was analysed by dissolving a 4.9 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 2.8 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample (Fe3O4 =231.54 g/mol, Fe2O3 = 159.69 g/mol)

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