6. a) It was obvious that most of you obtained a contaminated sample of beta naphthol. Look up the solubility of beta naphthol and benzoic acid in both cold and hot water. Will a single recrystallization with water be able to purify 1.0 gram beta naphthol (remove benzoic acid as an impurity). In other words, what is the minimum benzoic acid that beta naphthol can have above which more than one recrystallisation will be required. b) What would be a suitable recrystallisation solvent (or mixture of solvents) for beta naphthol? c) What is the minimum beta naphthol that could be present in benzoic acid above which a more than a single recrystallisation would be required?

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter84: Fractional Distillation, Azeotropes
Section: Chapter Questions
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6. a) It was obvious that most of you obtained a contaminated sample of beta
naphthol. Look up the solubility of beta naphthol and benzoic acid in both cold
and hot water. Will a single recrystallization with water be able to purify 1.0 gram
beta naphthol (remove benzoic acid as an impurity). In other words, what is the
minimum benzoic acid that beta naphthol can have above which more than one
recrystallisation will be required.
b) What would be a suitable recrystallisation solvent (or mixture of solvents) for
beta naphthol?
c) What is the minimum beta naphthol that could be present in benzoic acid
above which a more than a single recrystallisation would be required?
Transcribed Image Text:6. a) It was obvious that most of you obtained a contaminated sample of beta naphthol. Look up the solubility of beta naphthol and benzoic acid in both cold and hot water. Will a single recrystallization with water be able to purify 1.0 gram beta naphthol (remove benzoic acid as an impurity). In other words, what is the minimum benzoic acid that beta naphthol can have above which more than one recrystallisation will be required. b) What would be a suitable recrystallisation solvent (or mixture of solvents) for beta naphthol? c) What is the minimum beta naphthol that could be present in benzoic acid above which a more than a single recrystallisation would be required?
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