4000 100 80 IR Spectrum (liquid film) 20 % of base peak 40 10 3.0 3000 13C NMR Spectrum (125.0 MHZ, CDCI, solution) 77 DEPT CH₂ CH₂ CH₂ proton decoupled 200 ¹H NMR Spectrum (600 MHz, CDCI, solution) expansion 80 9 7.6 ppm 105 2000 8 M** 134 1690 V (cm¹) 160 $1 120 160 m/e www 7 1600 6 1200 200 240 120 Mass Spectrum expansions 800 5 C₂H100 280 solvent 80 1.1 ppm 4 0.0 0.5 1.0 1.5 absorbance 200 3 40 UV spectrum 1.075 mg/10 mls path length: 0.10 cm solvent: ethanol 250 2 300 λ (nm) 0 1 350 8 (ppm) TMS 0 8 (ppm)

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Given the following NMR data, find the unknown compound. 

a. Identify the molecular formula; find IHD
b. Identify the 1H and 13C NMR signals

4000
100
stedadadadadad
80
60
40
20
IR Spectrum
(liquid film)
% of base peak
10
8.0
3000
40
13C NMR Spectrum
(125.0 MHZ, CDCI, solution)
77
proton decoupled
DEPT CH₂ CH₂ CH4
¹H NMR Spectrum
(600 MHz, CDCI, solution)
expansion
9
200
80
7.6 ppm
105
8
2000
120
M+
134
Joy
My
1690
V (cm'¹)
160
7
m/e
160
1600
200
6
120
1200
240
800
Mass Spectrum
50
CgH100
280
solvent
expansions
I
3.1
2.9 1.3
80
1.1 ppm
4
0.0
0.5
1.0
1.5
absorbance
200
3
40
UV spectrum
1.075 mg / 10 mls
path length: 0.10 cm
solvent: ethanol
250
2
300
λ (nm)
0
1
350
8 (ppm)
TMS
0
8 (ppm)
Transcribed Image Text:4000 100 stedadadadadad 80 60 40 20 IR Spectrum (liquid film) % of base peak 10 8.0 3000 40 13C NMR Spectrum (125.0 MHZ, CDCI, solution) 77 proton decoupled DEPT CH₂ CH₂ CH4 ¹H NMR Spectrum (600 MHz, CDCI, solution) expansion 9 200 80 7.6 ppm 105 8 2000 120 M+ 134 Joy My 1690 V (cm'¹) 160 7 m/e 160 1600 200 6 120 1200 240 800 Mass Spectrum 50 CgH100 280 solvent expansions I 3.1 2.9 1.3 80 1.1 ppm 4 0.0 0.5 1.0 1.5 absorbance 200 3 40 UV spectrum 1.075 mg / 10 mls path length: 0.10 cm solvent: ethanol 250 2 300 λ (nm) 0 1 350 8 (ppm) TMS 0 8 (ppm)
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