Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Transcribed Image Text:Experimental Procedure
Part I: Making Crude Acetaminophen
1. Weigh 0.150 g of p-aminophenol and place this in a 5-mL conical vial.
2. Add 0.450 mL of water and 0.165 mL of acetic anhydride
3. Place a spin vane in the conical vial and attach an air condenser.
4. Heat the reaction mixture with an aluminum block or sand bath at about 115°C and stir gently.
5. After the solid has dissolved (it may dissolve, precipitate, and re-dissolve), heat the mixture
for an additional 20 minutes to complete the reaction.

Transcribed Image Text:4) what is the a method you can use to remove an
impurity? When will your method work or not
work?
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