32 Experiment 4: Separation Process Design The mixture of compounds you must design a separation process for is trans-Cinnamic acid +Cellulose See Blueline notes to complete the pre-lab assignment You will be provided ~1g of the mixture (containing 0.5g of each compound) on the day of lab. The table below provides solubility information of compounds to be separated: Solubility at 23 °C in Recrystallizes from Extracts into Compound 1M NAOH? CH2CL2 H2O Water Acetylsalicylic acid Y Sp. 00 Water Y Benzoic acid Sp. Ethanol Ins. Benzophenone Water Sp. N Caffeine Water Sp. Camphor Ins. Ins. N Cellulose* Ins. Water Cholesterol ОО Sp. Y Water trans-cinnamic acid ОО Water Sp. Menthol Water Y Sp. Salicylic acid Ethanol Y Sucrose Ins. 00 Water Y Sp. meta-toluic acid 00 Ins. - Insoluble Sp. Sparingly soluble 00 - Infinitely soluble *Purification procedure not required (cellulose only) Z CO
32 Experiment 4: Separation Process Design The mixture of compounds you must design a separation process for is trans-Cinnamic acid +Cellulose See Blueline notes to complete the pre-lab assignment You will be provided ~1g of the mixture (containing 0.5g of each compound) on the day of lab. The table below provides solubility information of compounds to be separated: Solubility at 23 °C in Recrystallizes from Extracts into Compound 1M NAOH? CH2CL2 H2O Water Acetylsalicylic acid Y Sp. 00 Water Y Benzoic acid Sp. Ethanol Ins. Benzophenone Water Sp. N Caffeine Water Sp. Camphor Ins. Ins. N Cellulose* Ins. Water Cholesterol ОО Sp. Y Water trans-cinnamic acid ОО Water Sp. Menthol Water Y Sp. Salicylic acid Ethanol Y Sucrose Ins. 00 Water Y Sp. meta-toluic acid 00 Ins. - Insoluble Sp. Sparingly soluble 00 - Infinitely soluble *Purification procedure not required (cellulose only) Z CO
Chemistry
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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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How can you separate trans-cinnamic acid from cellulose given the following information?

Transcribed Image Text:32
Experiment 4: Separation Process Design
The mixture of compounds you must design a separation process for is
trans-Cinnamic acid +Cellulose
See Blueline notes to complete the pre-lab assignment
You will be provided ~1g of the mixture (containing 0.5g of each compound) on the day of lab.
The table below provides solubility information of compounds to be separated:
Solubility at 23 °C in
Recrystallizes
from
Extracts into
Compound
1M NAOH?
CH2CL2
H2O
Water
Acetylsalicylic acid
Y
Sp.
00
Water
Y
Benzoic acid
Sp.
Ethanol
Ins.
Benzophenone
Water
Sp.
N
Caffeine
Water
Sp.
Camphor
Ins.
Ins.
N
Cellulose*
Ins.
Water
Cholesterol
ОО
Sp.
Y
Water
trans-cinnamic acid
ОО
Water
Sp.
Menthol
Water
Y
Sp.
Salicylic acid
Ethanol
Y
Sucrose
Ins.
00
Water
Y
Sp.
meta-toluic acid
00
Ins. - Insoluble
Sp. Sparingly soluble
00 -
Infinitely soluble
*Purification procedure not required (cellulose only)
Z
CO
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