2. What potential problem can a student have when an R₁ = 0 is obtained for an unknown sample on a silica TLC plate developed with a hexane mixture. How can this problem be avoided involving another TLC experiment?
2. What potential problem can a student have when an R₁ = 0 is obtained for an unknown sample on a silica TLC plate developed with a hexane mixture. How can this problem be avoided involving another TLC experiment?
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Transcribed Image Text:**Question 2: TLC Plate Analysis**
**Problem:**
What potential problem can a student encounter when an \( R_f = 0 \) is obtained for an unknown sample on a silica TLC plate developed with a hexane mixture?
**Solution:**
The issue here is that the compound did not move from the origin, indicating it is too polar to be eluted by the non-polar hexane solvent. To resolve this, consider using a more polar solvent or solvent mixture to increase compound movement during the TLC experiment.
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