2. In some cases, for very low energy electrons, k is rather short and a diffraction pattern may contain only Bragg beams corresponding to a particular planes of reciprocal space (e.g. look at the electron diffraction patterns in the lecture notes). An orthorhombic crystal has a = 0.45 nm, b = 0.15 nm and c = 0.20 nm. a) Construct and accurately draw (use graphing software if it helps) a section of the plane of reciprocal space containing a* and b* (i.e. the a*b* plane). (Your section should be large enough to allow you to complete parts c) and d)). (4) b) Indicate the relative orientation of the real space lattice vectors a, b and c relative to the unit vectors of the reciprocal lattice. (1) c) Suppose the crystal is now illuminated with a beam of electrons with wavevector k = -2a*-b*. Use the Ewald sphere construction to determine the allowed Bragg reflections in this plane of reciprocal space. Sketch the cross section of the Ewald sphere on your diagram and give the Miller indices for allowed reflections. (For TEM experts: For this analysis, assume the relrods are very small and ignore directional variations in the electron scattering due to the atomic scattering factor, f.). (6) d) On your diagram, draw and list in vector notation (i.e. g in terms of a*, b* and c*) the reciprocal lattice vectors, g, corresponding to the Bragg reflections. (3)

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2. In some cases, for very low energy electrons, k is rather short and a diffraction pattern may
contain only Bragg beams corresponding to a particular planes of reciprocal space (e.g. look at
the electron diffraction patterns in the lecture notes). An orthorhombic crystal has a = 0.45 nm,
b = 0.15 nm and c = 0.20 nm.
a) Construct and accurately draw (use graphing software if it helps) a section of the plane of
reciprocal space containing a* and b* (i.e. the a*b* plane). (Your section should be large
enough to allow you to complete parts c) and d)).
(4)
b) Indicate the relative orientation of the real space lattice vectors a, b and c relative to the unit
vectors of the reciprocal lattice.
(1)
c) Suppose the crystal is now illuminated with a beam of electrons with wavevector k = -2a*-b*.
Use the Ewald sphere construction to determine the allowed Bragg reflections in this plane of
reciprocal space. Sketch the cross section of the Ewald sphere on your diagram and give the
Miller indices for allowed reflections. (For TEM experts: For this analysis, assume the relrods are
very small and ignore directional variations in the electron scattering due to the atomic
scattering factor, f.).
(6)
d) On your diagram, draw and list in vector notation (i.e. g in terms of a*, b* and c*) the
reciprocal lattice vectors, g, corresponding to the Bragg reflections.
(3)
Transcribed Image Text:2. In some cases, for very low energy electrons, k is rather short and a diffraction pattern may contain only Bragg beams corresponding to a particular planes of reciprocal space (e.g. look at the electron diffraction patterns in the lecture notes). An orthorhombic crystal has a = 0.45 nm, b = 0.15 nm and c = 0.20 nm. a) Construct and accurately draw (use graphing software if it helps) a section of the plane of reciprocal space containing a* and b* (i.e. the a*b* plane). (Your section should be large enough to allow you to complete parts c) and d)). (4) b) Indicate the relative orientation of the real space lattice vectors a, b and c relative to the unit vectors of the reciprocal lattice. (1) c) Suppose the crystal is now illuminated with a beam of electrons with wavevector k = -2a*-b*. Use the Ewald sphere construction to determine the allowed Bragg reflections in this plane of reciprocal space. Sketch the cross section of the Ewald sphere on your diagram and give the Miller indices for allowed reflections. (For TEM experts: For this analysis, assume the relrods are very small and ignore directional variations in the electron scattering due to the atomic scattering factor, f.). (6) d) On your diagram, draw and list in vector notation (i.e. g in terms of a*, b* and c*) the reciprocal lattice vectors, g, corresponding to the Bragg reflections. (3)
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