1. If all the impurities in a certain sample are soluble in the solvent being used, would it be necessary to do a hot filtration? Explain why or why not. 2. Use the following solubility data to answer all parts of this question. You can assume that the presence of one compound in solution does not affect or change the solubility of another compound in that same solution. Compound Benzoic acid Impurity Solubility in water at 25°C 0.34 grams per 100 mL of water 0.50 grams per 100 mL of water A. Will 5.7 grams of benzoic acid dissolve in 100 mL of water at 95°C? B. If 4.50 grams of benzoic acid are dissolved in 100 mL of hot water and then allowed to cool to 25°C followed by vacuum filtration, how many grams of benzoic acid crystals would be obtained? Show your work. Solubility in water at 95°C 6.81 grams per 100 mL of water 4.25 grams per 100 mL of water What percentage of the original benzoic acid sample is this? In other words, what is your percent recovery of benzoic acid crystals? Show your work. I to 224

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Recrystallization of Acetanilide: POSTLAB
1. If all the impurities in a certain sample are soluble in the solvent being used, would it
be necessary to do a hot filtration? Explain why or why not.
2. Use the following solubility data to answer all parts of this question. You can assume
that the presence of one compound in solution does not affect or change the solubility
of another compound in that same solution.
3.
Compound
Benzoic acid
Impurity
Solubility in water at 25°C
0.34 grams per 100 mL of water
0.50 grams per 100 mL of water
A. Will 5.7 grams of benzoic acid dissolve in 100 mL of water at 95°C?
B. If 4.50 grams of benzoic acid are dissolved in 100 mL of hot water and then allowed
to cool to 25°C followed by vacuum filtration, how many grams of benzoic acid
crystals would be obtained? Show your work.
Solubility in water at 95°C
6.81 grams per 100 mL of water
4.25 grams per 100 mL of water
What percentage of the original benzoic acid sample is this? In other words, what
is your percent recovery of benzoic acid crystals? Show your work.to
C. A sample of impure benzoic acid has a mass of 6.00 grams. This sample consists of
4.50
grams of benzoic acid and 1.50 grams of the impurity listed in the table above.
Suppose that this 6.00 gram sample is dissolved in 100 mL of water at 95°C and
then allowed to cool to room temperature (about 25°C). The crystals that form are
then filtered out.
Are these crystals pure benzoic acid?
To be sure you have answered correctly, complete the following two calculations.
ow wode
How many grams of benzoic acid will crystallize when the solution has cooled?
Show your work.
How many grams of the impurity will crystallize when the solution has cooled?
Show
your work.
Transcribed Image Text:Recrystallization of Acetanilide: POSTLAB 1. If all the impurities in a certain sample are soluble in the solvent being used, would it be necessary to do a hot filtration? Explain why or why not. 2. Use the following solubility data to answer all parts of this question. You can assume that the presence of one compound in solution does not affect or change the solubility of another compound in that same solution. 3. Compound Benzoic acid Impurity Solubility in water at 25°C 0.34 grams per 100 mL of water 0.50 grams per 100 mL of water A. Will 5.7 grams of benzoic acid dissolve in 100 mL of water at 95°C? B. If 4.50 grams of benzoic acid are dissolved in 100 mL of hot water and then allowed to cool to 25°C followed by vacuum filtration, how many grams of benzoic acid crystals would be obtained? Show your work. Solubility in water at 95°C 6.81 grams per 100 mL of water 4.25 grams per 100 mL of water What percentage of the original benzoic acid sample is this? In other words, what is your percent recovery of benzoic acid crystals? Show your work.to C. A sample of impure benzoic acid has a mass of 6.00 grams. This sample consists of 4.50 grams of benzoic acid and 1.50 grams of the impurity listed in the table above. Suppose that this 6.00 gram sample is dissolved in 100 mL of water at 95°C and then allowed to cool to room temperature (about 25°C). The crystals that form are then filtered out. Are these crystals pure benzoic acid? To be sure you have answered correctly, complete the following two calculations. ow wode How many grams of benzoic acid will crystallize when the solution has cooled? Show your work. How many grams of the impurity will crystallize when the solution has cooled? Show your work.
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