Answered: 1. For each separatory funnel below,… | bartleby

Fundamentals Of Analytical Chemistry

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter9: Aqueous Solutions And Chemical Equilibria

Section: Chapter Questions

Problem 9.20QAP

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1) need help

1. For each separatory funnel below, match the compounds to the left of the funnel
with the proper phase on the right of the funnel. Hint: How do you know which
solvent will be on top?
Example:
H
H.
water
Br
Top layer
Bottom layer
H.
benzene
Br
bromobenzene
NH2
diethyl ether
4-chloroaniline
H-CI
HH
Top layer
Top layer
hydrochloric acid
water
Bottom layer
Bottom layer
HH
HO,
water
H
it
benzoic acid
CI
CI
dichloromethane

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Provide the species or reagents needed to complete the reaction map. Refer to the following choices. OH H₂ Bra Cl₂ H₂O A Bra CH₂Cl₂ B 1) 080₁ 2) NaHSO₂, H₂O с Pd/C H₂O D E **&& Bad HO OH da H K M (2) (1) 1) BH,, THF 2) H₂O₂, OH- CI OH Ga Br Br - OH 1) Hg(OAc) H₂O/THF 2) NaBH, (10) (9) OH un (8) mCPBA CH₂Cl₂ H₂O* (6) (7) (3) 1) 0₂ 2) Zn, H₂O KMnO H₂O* (5)
10. E to CH3ONa a) Br₂ Br2 1. Mg /ether khan (A) (B) (C) (D) hv FeBr3 hv 2. CO2 3. H3O+ C1 B2 B3 B1 KMnO4 H+ C1 Mg, ether CHO b) 1. CH3Mgl H2SO4 HBr 1. Mgether khan A B D to 2. H3O+ peroxide 2. H₂C-CH2 ° CH3COCI AICI 3 1. C1 1. 03 G F E 2. H3O+ 2. Na₂S 3. H3O+
Need help with both questions, please!
Give Clear Detailed Solution with explanation needed ..don't give Handwritten answer
3. Draw the structure(s) of the major organic product(s), for each of the following reactions. ELOH cat. H,SO, Br 1) 2 eq. Li b) 2) PHCHO 3) NH,C(ag) Ph = Phenyl 2 oq. Li c) NH,(1) 1) Hg(O,CCF3)z, (CH,);COH d) 2) NABH,, NAOH cat. NMO CH;C),
In each reaction box, place the best reagent and conditions from the list provided. 1) Br 2) 3) 4) DEET (the active ingredient in over the counter insect repellant) 5) Answer Bank Mg, Et,0 HN(CH, CH, ), (1 equiv.) H,O* CH,COOH CH,CH,NH, CH,CH, Br NH(CH,CH,),(2 cquiv.) НСООСH, H,CO НСООН CH, CH, OH NaCN NaNH, Br,, FeBr, SOCI, CO,
7 Best reuyent choice ? -> Br Br ota Pd 0) Fe H,0", 2) NaOHL ONz Hy Nu OH 18 Bar reaynt choice Z 7 HO 01) N.OCH2CH3,2)CICH 2CH2CH2C1,3)MOCH2 CH 3, 4204, heat H Na OCH,CH2, 2) CH3 CHz CHZBC, 3) tH;O" , heat 01 01/N0CHli3CHq,2) CHy =CHICH4,CH =0, 3) Hy O", heut
The following syntheses have flaws. What is wrong with each?
Answer questions a-c about the Bronsted acid-base reaction below using the identifying letters A-D below each structure. A table of pK, values for various organic and inorganic acids can be found in the references section. CH₂ -NH3 A ethylammonium + CH₂ B ethoxide CH₂ "NH₂ + CH₂ C ethylamine a) The weaker base is b) Its conjugate acid is c) The species that predominate at equilibrium are (two letters, e.g. AC) OH D ethanol
The blcyclic ketone shown below is first treaterd with a base, then ethyliodide is added to form the substituted ketone. Which base/conditions are sultable? 1) Base 2) O 1. Lithium diisopropylamide in THF at -78 "C. O 2. NaBH4 in methanol at room temperature. O 3. Sodium methoxide in methanol at room temperature. O 4. DBU in THF at 25 "C.
Answer questions a-c about the Bronsted acid-base reaction below using the Q41 identifying letters A-D below each structure. A table of pk, values for various organic and inorganic acids can be found in the references section. NH₂ A amide B ethyl acetate CH₂ NH3 C ammonial + I CH₂ D ethyl acetate enolate a) The weaker acid is b) Its conjugate base is c) The species that predominate at equilibrium are (two letters, e.g. AC)
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