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1. DMAP (cat.) THF, rt R. ОМОМ HO 2. Ai203, 60 °C R = (CH2)3OBN

1. DMAP (cat.) THF, rt R. ОМОМ HO 2. Ai203, 60 °C R = (CH2)3OBN

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Explain the mechanisms of the reactions
1. DMAP (cat.) THF, rt R. ОМОМ Но 2. Ai2O3, 60 °C R = (CH2)3OBN %3D
Transcribed Image Text:1. DMAP (cat.) THF, rt R. ОМОМ Но 2. Ai2O3, 60 °C R = (CH2)3OBN %3D
1a. n-BuLi, THF, -78 °C 1b. Cul (0.5 eq) 1c. allyl bromide (0.5 eq) -78 °C to rt SPh 2a. MeOSO2F (neat) 2b. triturate with pentane 3. KOH (s) (4 eq), DMSO, RT 56%
Transcribed Image Text:1a. n-BuLi, THF, -78 °C 1b. Cul (0.5 eq) 1c. allyl bromide (0.5 eq) -78 °C to rt SPh 2a. MeOSO2F (neat) 2b. triturate with pentane 3. KOH (s) (4 eq), DMSO, RT 56%
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