1- Prepare 0.010 M sodium thiosulphate in 250.0-ml vol.flask. 2- Prepare 0.40 M sodium acetate in 250.0-ml vol.flask 3- Prepare 1.0 M Cl₂CHCOOH in 100-ml vol.flask. 4- Prepare 0.050 M iodine (in 10% KI) in 100 ml vol.flask.

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Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Q) Explain how to prepare
this experiment by drawing?
..1- Prepare 0.010 M sodium thiosulphate in 250.0-ml vol.flask.
2- Prepare 0.40 M sodium acetate in 250.0-ml vol.flask
.
3- Prepare 1.0 M Cl₂CHCOOH in 100-ml vol.flask.
4- Prepare 0.050 M iodine (in 10% KI) in 100 ml vol.flask.
** Prepare the following solution in 100-ml vol.flask.
Sol. Volume of 1.0 M
No.
1
2
Sol.
No.
1
Cl₂CHCOOH
(ml)
5.0
2
10.0
Interval between
samples (min)
10
Water
(ml)
6
78.0
* Shake and clamp in the thermostat at 25°C, for about 15
minutes. Then add 10.0 ml of 0.05 Iodine (in KI) solution which
has brought to 25°C, then complete the vol.flask to the mark by
water and start stopclock.
Tip the solution into a 250-ml Erlenmeyer flask and clamp this
solution in the thermostat.
73.0
Volume of
acetone
(ml)
2.0
2.0
Volume of
0.40 M NaAc
5.0
10.0
*Take 10.0 ml from each solution then add volume of 0.40 M
NaAc and titrate with 0.010 M sodium thiosulphate (use the
starch as indicator), Take 6 samples in each solution for the
same interval between samples.
Transcribed Image Text:Q) Explain how to prepare this experiment by drawing? ..1- Prepare 0.010 M sodium thiosulphate in 250.0-ml vol.flask. 2- Prepare 0.40 M sodium acetate in 250.0-ml vol.flask . 3- Prepare 1.0 M Cl₂CHCOOH in 100-ml vol.flask. 4- Prepare 0.050 M iodine (in 10% KI) in 100 ml vol.flask. ** Prepare the following solution in 100-ml vol.flask. Sol. Volume of 1.0 M No. 1 2 Sol. No. 1 Cl₂CHCOOH (ml) 5.0 2 10.0 Interval between samples (min) 10 Water (ml) 6 78.0 * Shake and clamp in the thermostat at 25°C, for about 15 minutes. Then add 10.0 ml of 0.05 Iodine (in KI) solution which has brought to 25°C, then complete the vol.flask to the mark by water and start stopclock. Tip the solution into a 250-ml Erlenmeyer flask and clamp this solution in the thermostat. 73.0 Volume of acetone (ml) 2.0 2.0 Volume of 0.40 M NaAc 5.0 10.0 *Take 10.0 ml from each solution then add volume of 0.40 M NaAc and titrate with 0.010 M sodium thiosulphate (use the starch as indicator), Take 6 samples in each solution for the same interval between samples.
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