III. Experimental Data Table 3b.1. Observation on determination of melting point of unknown A. Appearance of Sample in Capillary Tube Appearance of Sample in Capillary Tube Temperature, °C Temperature, °C solid 120.0 liquid solid ... 114.0 solid 120.5 liquid solid 116.0 solid 121.0 liquid solid| 117.0 solid 121.0 liquid solid 118.0 solid 121.0 liquid solid 119.0 appearance of first liquid 121.5 liquid solid 119.5 solid liquid 122.0 liquid 120.0 solid liquid 123.0 liquid 120.0 solid liquid liquid Table 3b.2. Observation on determination of melting point of unknown B. Appearance of Sample in Capillary Appearance of Sample in Capillary Tube Temperature, °C Temperature, °C Tube solid 79.0 liquid solid ... 72 solid 79.5 liquid solid 73 solid 79.5 liquid solid 74 solid 80.0 liquid solid 76 solid 80.0 liquid solid 78.0 appearance of first liquid 80.0 liquid solid 78.0 solid liquid 82.0 liquid 78.5 solid liquid 84.0 liquid 79.0 solid liquid 86.0 liquid 79.0 solid liquid liquid

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Table 3.2

 

Kindly find the following and use the data provided.

Table 3b.2. Determination of the melting point range, experimental melting point and posible identity of unknowns A and B.
Unknown A
Unknown B
Parameters
Melting Point Range
Experimental Melting Point
Possible Identity
Percent Error, % (Melting Point)
Transcribed Image Text:Table 3b.2. Determination of the melting point range, experimental melting point and posible identity of unknowns A and B. Unknown A Unknown B Parameters Melting Point Range Experimental Melting Point Possible Identity Percent Error, % (Melting Point)
III. Experimental Data
Table 3b.1. Observation on determination of melting point of unknown A.
Temperature, °C
Appearance of
Sample in Capillary
Tube
Appearance of
Sample in Capillary
Tube
Temperature, °C
solid
120.0
liquid solid
...
114.0
solid
120.5
liquid solid
116.0
solid
121.0
liquid solid|
117.0
solid
121.0
liquid solid
118.0
solid
121.0
liquid solid
119.0
appearance of first liquid
121.5
liquid solid
119.5
solid liquid
122.0
liquid
120.0
solid liquid
123.0
liquid
120.0
solid liquid
liquid
...
Table 3b.2. Observation on determination of melting point of unknown B.
Appearance of
Sample in Capillary
Tube
Appearance of
Sample in Capillary
Temperature, °C
Temperature, °C
Tube
solid
79.0
liquid solid
72
solid
79.5
liquid solid
73
solid
79.5
liquid solid
74
solid
80.0
liquid solid
76
solid
80.0
liquid solid
78.0
appearance of first liquid
80.0
liquid solid
78.0
solid liquid
82.0
liquid
78.5
solid liquid
84.0
liquid
79.0
solid liquid
86.0
liquid
79.0
solid liquid
liquid
...
Transcribed Image Text:III. Experimental Data Table 3b.1. Observation on determination of melting point of unknown A. Temperature, °C Appearance of Sample in Capillary Tube Appearance of Sample in Capillary Tube Temperature, °C solid 120.0 liquid solid ... 114.0 solid 120.5 liquid solid 116.0 solid 121.0 liquid solid| 117.0 solid 121.0 liquid solid 118.0 solid 121.0 liquid solid 119.0 appearance of first liquid 121.5 liquid solid 119.5 solid liquid 122.0 liquid 120.0 solid liquid 123.0 liquid 120.0 solid liquid liquid ... Table 3b.2. Observation on determination of melting point of unknown B. Appearance of Sample in Capillary Tube Appearance of Sample in Capillary Temperature, °C Temperature, °C Tube solid 79.0 liquid solid 72 solid 79.5 liquid solid 73 solid 79.5 liquid solid 74 solid 80.0 liquid solid 76 solid 80.0 liquid solid 78.0 appearance of first liquid 80.0 liquid solid 78.0 solid liquid 82.0 liquid 78.5 solid liquid 84.0 liquid 79.0 solid liquid 86.0 liquid 79.0 solid liquid liquid ...
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