Mark this Report - Uncertainty Lab

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Industrial Engineering

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Dec 6, 2023

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Material Identification by Density Course: PCS-211 Section 7 Instructor: Dr. Eric Da Silva TA: Diana Ha Date of Submission: September 17, 2023 Performed by: Ammar Siddiqui and Shayan Hajizad
Introduction The purpose of this lab was to identify an unknown material which was given in the form of a cuboid block. The volume of the material was measured using three distinct methods. Each different method yielded three different volume values. These volumes were used to calculate three different densities. By comparing the average density to a table of known values, the unknown material was identified. This lab also accounted for the uncertainty of each measuring method. The uncertainties were utilized to determine the consistency of the results. Theory There were two core physics concepts investigated in this lab, uncertainty in physics, and density of materials. Uncertainty In physics, it is important to show that the tool used has some sort of uncertainty associated with it. When expressing a measured value, x, then the measured value should be written in the following way, , 𝑥 ± ∆𝑥 where is the associated uncertainty. ∆𝑥 Any measuring device is limited by the process it was manufactured. No process of manufacturing is perfect. Due to this, when reporting measurements taken with instruments, the associated uncertainty is the smallest increment of that tool divided by two. Calculating the mean value of measurements makes sure that the results are consistent. In this lab, the mean value of the densities is calculated using the following formula, (µ) (1) µ = ??? ?? ???????? ?????? ?????? ?? ?????? When performing calculations with uncertain measurements, in this case addition/subtraction followed by multiplication/division the following two rules are followed, (2) ∆? = ∆? 2 + ∆? 2 (3) ∆? ? = ( ∆? ? ) 2 + ( ∆? ? ) 2 where , are the measurements and is the result of the operation. , , and are the ? ? ? ∆? ∆? ∆? associated uncertainties with their respective measurements. Density of Materials Density is a measure of how much mass is present in a given amount of volume. The SI unit of density is kg/m 3 (kilograms per cubic meter). The closer the particles in a substance are packed together, the higher its density. Materials with uniform properties exhibit clearly defined densities, making them distinguishable based on their density. The quality of uniform materials
having unique densities can be used to ascertain its identity. The density of a material (ρ) can be determined by using the formula, ρ = , (4) ? ? where stands for the measured volume of the material and stands for the measured mass of ? ? the material (1) . Procedure A glass beaker, a graduated cylinder, a standard metre stick, a vernier caliper, a triple beam balance, and one unknown material were used in the following procedure. The mass of the unknown material was measured using the triple beam balance. The counter masses were adjusted so that the beam was balanced and a reading of the measurement was recorded. The uncertainty of the triple beam balance was 0.05g. ± The metre stick was then used to measure the dimensions of the unknown material, including the length, width, and height. The uncertainty of the metre stick was 0.1 cm. These values were ± later used to calculate the volume of the block. Next, the vernier caliper was used to measure the dimensions of the unknown material, including the length, width, and height. The uncertainty of the caliper was 0.005 cm. These values were ± later used to calculate the volume of the block. Lastly, the method of water displacement was used to measure the volume of the unknown material. A beaker was used to measure out 300 mL of water. The unknown material was then placed inside of the beaker. Next, the water was poured out of the beaker into a graduated cylinder until the reading on the beaker was 300 mL. The graduated cylinder gives a more accurate reading of the volume displaced with an uncertainty of 1 mL. ±
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Results and Calculations It is known that when dealing with water, and Volume, (2) . 1? = 1?? 3 ? = 𝐿 * ? * 𝐻 Table 1: Summary of dimensions and mass of block, including calculations for volumes, density, and average density. [See Appendix A for data.] Metre Stick Uncertainty Vernier Caliper Uncertainty Volume Displacement Uncertainty Volume (cm 3 ) 12 0.6 10.8 0.05 12 0.5 Density (g/cm 3 ) 9.5 0.4 11.0 0.05 9.9 0.4 Average Density (g/cm 3 ) 10. 1 Sample Calculations (Metre Stick): Volume ? = 𝐿 * ? * 𝐻 ? = 3. 1 * 3. 1 * 1. 3 ? = 12. 493 ?? 3 Uncertainty Using equation (3) ∆? = ( 0.05 3.1 ) 2 + ( 0.05 3.1 ) 2 + ( 0.05 1.3 ) 2 * 12. 493 ∆? = 0. 55864546 ?? 3 Therefore ? = 12 ± 0. 6 ?? 3 Density Using equation (4)
ρ = 118.5 ? 12.493 ?? 3 ρ = 9. 485311775 ?/?? 3 Uncertainty Using equation (3) ∆? = ( 0.05 118.5 ) 2 + ( 0.55864546 12.493 ) 2 * 9. 485311775 ∆? = 0. 4241705156 ?/?? 3 Therefore ρ = 9. 5 ± 0. 4 ?/?? 3 Average Density Using equation (1) µ = 9.5 + 9.9 + 11.0 3 µ = 10. 13 Uncertainty Using equation (2) ∆? = 0. 9 2 + 0. 05 2 + 0. 8 2 ∆? = 1. 205197079 Therefore the average density which is used for conclusions, ρ = 1. 0 ± 0. 1 * 10 1 ?/?? 3 By using the average of the density values obtained using multiple methods, accuracy and precision can both be addressed. Accuracy is improved because the potential biases and errors introduced by each measurement method is reduced. This makes the final result closer to the actual true value. Precision is improved because the consistency of results obtained from different methods indicates that the measurements are reproducible. It also checks for the uncertainties of each of the different measurement methods. (3)
Discussion and Conclusion Material Identification: 1. Metre Stick: According to the calculations, the density of the material is . This density is closest to the density of copper. [see ρ = 9. 5 ± 0. 4 ?/?? 3 Appendix B] % ????? = 9.5 − 8.96 8.96 | | | | · 100% = 6. 03% 2. Vernier Caliper: According to the calculations, the density of the material is . This density is closest to the density of silver. [see ρ = 11. 0 ± 0. 05 ?/?? 3 Appendix B] % ????? = 11.0 − 10.49 10.49 | | | | · 100% = 4. 86% 3. Volume Displacement: According to the calculations, the density of the material is . This comes closest to the density of silver. [see Appendix ρ = 9. 9 ± 0. 4 ?/?? 3 B] % ????? = 9.9 − 10.49 10.49 | | | | · 100% = 5. 62% In this lab, the uncertainty of the measurements were defined only by the measurement instruments. The following are other possible sources of uncertainty that could have had an impact on the results: 1. Human Error: Parallax errors in reading instruments, inconsistent hand movements, and/or misreadings of the results can introduce major uncertainty. In this experiment, the results relied heavily on human measurements, so this must have had quite a significant impact on the final results. 2. Calibration Uncertainty: The instruments used in this experiment were calibrated beforehand. However, there is a high likelihood that the instruments, mainly the triple beam balance, were incorrectly calibrated. This uncertainty heavily affects the accuracy of the results (4) . Percent error and uncertainty are both used in scientific experiments to convey to the reader how accurate the results found were. Uncertainty quantifies the range of possible values in which the true value may lie. It properly expresses the variability in the measured and calculated data. Percent error, on the other hand, expresses how far off the experimentally calculated value is from the true value. It is calculated using the following formula: % ????? = ???????? ????? − ???? ????? ???? ????? | | | | · 100% Percent error provides an insight into the accuracy of the measurements and shows how close or far away the results are from an expected value. It is important to calculate the percent error
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because it assesses the accuracy of the measurement tools and methods. A high percent error indicates that there are significant errors in the experiment (5) . The average density found in this experiment is . ρ = 1. 0 ± 0. 1 * 10 1 ?/?? 3 This is closest to the accepted value for the density of silver which is [see ρ = 10. 49 ?/?? 3 Appendix B]. Due to time constraints, there was only one trial performed for each of the measurement methods. However, looking at the percent error for each method, it seems that the vernier caliper is the most accurate method of measuring the dimensions of the block which had a percent error of only 4.86% . To conclude, the unknown block was silver.
References: (1) Britannica, T. Editors of Encyclopaedia (2023, July 4). density. Encyclopedia Britannica. https://www.britannica.com/science/density (2) Aqua-Calc. (n.d.). Weight to Volume Calculator for Water. Aqua-Calc. https://www.aqua-calc.com/calculate/weight-to-volume/substance/water (3) Accuracy, Precision, and Significant Figures. LibreTexts. https://chem.libretexts.org/Courses/Ontario_Tech_University/OTU-_Chemistry_1010/01 %3A_Chemical_Tools-_Experimentation_and_Measurement/1.09%3A_Accuracy_Precis ion_and_Significant_Figures (4) Helmenstine, A. (2016, November 3). Error in Science. Science Notes. https://sciencenotes.org/error-in-science/ (5) Jim Frost. (n.d.). Percent Error. Statistics by Jim. https://statisticsbyjim.com/basics/percent-error/
Appendix A - Dimensions of block Table 1A: Recorded values of the dimensions of the block and mass. Mass ( 0.05 g) ± Length (L) Width (W) Height (H) Volume Metre Stick ( 0.05 cm) ± 118.5 3.1 3.1 1.3 Vernier Caliper ( 0.005 cm) ± 3.06 3.06 1.15 Volume Displacement ( 0.5 mL) ± 12 Appendix B - Density of Common Substances [see Lab Manual] Material Density (g/cm 3 ) Titanium 4.50 Zinc 7.13 Tin 7.28 Iron 7.87 Brass 8.4 - 8.7 Copper 8.96 Silver 10.49 Lead 11.36
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